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发明授权
CN101031576B 叠氮基三甲基硅烷的制备方法 失效 - 权利终止

叠氮基三甲基硅烷的制备方法
摘要：
本发明涉及由式(3)表示的叠氮基三甲基硅烷的制备方法，其包括在相转移催化剂和高沸点有机溶剂的存在下，将由式(1)表示的氯化三甲基硅烷与由式(2)表示的叠氮化氢的无机盐反应，并且n表示1或2。(CH3)3SiCl(1)，M(N3)n(2)[其中M表示碱金属或碱土金属]，(CH3)3SiN3(3)。
摘要（英）：

The present invention relate to a method for producing a trimethylsilyl azide represented by the formula (3): (CH 3 ) 3 SiN 3 (3) which comprises reacting a trimethylsilyl chloride represented by the formula (1): (CH 3 ) 3 SiCl (1) with an inorganic salt of hydrogen azide represented by the formula (2): M(N 3 ) n (2) wherein M represents an alkali metal or an alkaline earth metal, and n represents 1 or 2, in the presence of a phase-transfer catalyst and an organic solvent having a high boiling point.

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