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CN101762667A 一种用于检测香豆素系化合物的方法 失效 - 权利终止

一种用于检测香豆素系化合物的方法
摘要：
本发明提供了一种用于检测香豆素系化合物的方法，该方法包括对样品进行超高效液相色谱和串联质谱检测，从而确定样品含有的香豆素系化合物的种类和含量。所述香豆素系化合物为醋硝香豆素、双香豆素、6-甲氧基-7-羟基香豆素、7-羟基香豆素、8-羟基补骨脂素、4-甲基-7-羟基香豆素、6，7-二甲氧基香豆素、香豆素、7-甲氧基香豆素、二氢香豆素、补骨脂素、异补骨脂素、8-甲氧基补骨脂素、7-甲基香豆素、5-甲氧基补骨脂素、4-甲基-7-乙氧基香豆素、4-甲基-7-二乙氨基香豆素、2′，4，8-三甲基补骨脂素、欧前胡素、异欧前胡素、二氢欧山芹醇当归酸酯和环香豆素中的一种或多种。本发明的方法可以在4分钟内完成22种香豆素系化合物的分析检测。
摘要（英）：

The invention provides a method for detecting coumarin series compounds, which comprises the following steps that: ultra high-efficiency liquid chromatography and tandem mass spectrometry detection are carried out to a sample, so as to determine the types and the content of coumarin series compounds contained in the sample. The coumarin series compounds comprise one or more types in vinegar Glass coumarin, dicoumarol, 6-methoxy-7-hydroxy coumarin, 7-hydroxycoumarin, 8-hydroxy-psoralen, 4-methyl-7-hydroxy coumarin, 6,7-dimethoxy coumarin, coumarin, 7-methoxy coumarin, dihydro coumarin, psoralen, psoralen, 8-methoxypsoralen, 7-methyl, 5-methoxypsoralen, 4-methyl-7-ethoxyl coumarin, 4-methyl-7-diethylamino coumarin, 2', 4,8-trimethyl psoralen, imperatorin, isoimperatorin, columbianadin and cyclocoumarol. The method of the invention can complete the analysis and the detection of 22 coumarin series compounds within 4 min.

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