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发明公开
CN104730193A 一种稳心颗粒中挥发性成分的检测方法 有权

一种稳心颗粒中挥发性成分的检测方法
摘要：
本发明提供一种稳心颗粒中挥发性成分的检测方法。本发明采用顶空固相微萃取技术，提取稳心颗粒中挥发性成分。并结合利用气相色谱-质谱联技术，共分离鉴定出挥发性成分74个。对10批稳心颗粒进行了分析，得出了主要挥发性成分的相对含量范围。本发明首次采用顶空固相微萃取结合气相色谱-质谱联用法，对稳心颗粒中挥发性成分进行提取与分析，弥补了以往对稳心颗粒挥发性物质分析的不足，为该药品的质量控制提供更为全面的检测方法。
摘要（英）：

The invention provides a detection method of a volatile component in heart stabilizing particles. By adopting a head space solid phase microextraction technology, the volatile component in the heart stabilizing particles can be extracted. By utilizing a gas chromatography and mass spectrum combined technology, the volatile component 74 can be isolated and identified together; 10 batches of heart stabilizing particles are analyzed, the relative content range of the main volatile component can be acquired. The head space solid phase microextraction technology is combined with the gas chromatography and mass spectrum combined technology for the first time, and the volatile components in the heart stabilizing particles are extracted and analyzed, so that the defects of analysis on the volatile components of the heart stabilizing particles are overcome, and a comprehensive detection method is provided for quality control of medicines.

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