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CN105602140A 一种用于鞋底材料的发光复合材料的制备方法 失效 - 放弃专利权

一种用于鞋底材料的发光复合材料的制备方法
摘要：
本发明提供一种用于鞋底材料的发光复合材料的制备方法，其大致步骤如下：(1)将硝酸锆、硝酸钡、硝酸镧、钛酸丁酯通过水热法制成复合发光粉体；(2)将步骤(1)得到的复合发光粉体通过偶联剂KH560改性处理，制成改性复合发光粉体，再将其与含氢聚硅氧烷、二月桂酸二丁基锡、偶联剂A151反应，得到聚硅氧烷接枝复合发光粉体；(3)将60-70重量份基体、1-2重量份润滑剂、1.5-2重量份稳定剂、3-4重量份相容剂、2-3重量份流动促进剂以及10-14重量份聚硅氧烷接枝复合发光粉体加入高混机混合，得到混合料；(4)将混合料加入双螺杆挤出机中熔融挤出，得到用于鞋底材料的发光复合材料。本发明制备出的鞋底材料具有较好的发光性能，可用于发光鞋。
摘要（英）：

The invention provides a preparation method of a luminous composite for a sole material. The preparation method roughly includes following steps: (1), using zirconium nitrate, barium nitrate, lanthanum nitrate and butyl titanate to prepare composite luminous powder through a hydrothermal method; (2), modifying the composite luminous powder obtained in the step (1) through a coupling agent KH560 to obtain modified composite luminous powder, and enabling the modified composite luminous powder to react with hydrogen-containing polysiloxane, dibutyltin dilaurate and a coupling agent A151 to obtain polysiloxane grafted composite luminous powder; (3), adding, by weight, 60-70 parts of matrix, 1-2 parts of lubricant, 1.5-2 parts of stabilizer, 3-4 parts of compatilizer, 2-3 parts of flowing promoter and 10-14 parts of the polysiloxane grafted composite luminous powder into a high mixer to obtain a mixture; (4), adding the mixture into a double-screw extruder for melt extrusion to obtain the luminous composite for the sole material. The sole material prepared by the method has high luminosity and can be used for luminous shoes.

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