The invention discloses an implosion emergency disposal method for mixed liquor of vinyl acetate and acetic acid. The method comprises the steps that firstly, vinyl acetate in the mixed liquor is divided into four zones according to mass percentage concentration, then thermodynamics data in each zone is determined according to the divided zones in combination with thermodynamics analysis, and emergency disposal temperature is determined according to the state of the mixed liquor, that is, when the mixed liquor is in a storage state, the temperature corresponding to the time TMRad equal to 24 h needed by the mixed liquor reaching the maximum reaction rate under the adiabatic condition is determined as emergency disposal temperature; when the mixed liquor is in the running process, the temperature corresponding to the time TMRad equal to 6 h needed by the mixed liquor reaching the maximum reaction rate under the adiabatic condition is determined as the emergency disposal temperature; finally, a cooling measure is taken to prevent the reaction from being out of control according to the emergency disposal temperature. According to the method, the safety control measures of vinyl acetate with different concentrations are adjusted, and therefore safety production is achieved.