The invention provides a separation method for chromium zirconium copper waste. The method mainly includes 1, a acid-pickling process, 2, a passivation process, 3, an oxidation process, 4, an absorption process, 5, a filtration process, 6, a concentration process, 7, a crystallization process, 8, a filtration process, 9, a drying process, 10, a rolling process, 11, an air separation and ash removal process, and 12, a packaging process. According to the method, the chromium zirconium copper waste can be separated, compared with a direct oxidation method in the past, through the method, a pure chromium zirconium alloy can be obtained through recycling, purer copper sulfate is obtained, the purity of the obtained copper sulfate can reach the industrial first grade, and the method has both environmental significance and economic significance.