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发明授权
CN1982320B 有机钼化合物的制备方法 有权 转让

有机钼化合物的制备方法
摘要：
本发明为通过将二醇-、二氨基-、巯基-醇-与氨基-醇-化合物与如下试剂反应制备2，4-杂原子-取代的氧化钼-3，3-二氧环烷烃的方法：以钼酸铵作为钼源(或者通过氨与三氧化钼或钼酸的反应就地产生钼酸铵)，以氨作为助剂或第二试剂或促进剂，NH3∶Mo(所述钼源中钼的量)的摩尔比为≥1∶1，优选为1-3∶1，更优选为2-3∶1，且最优选为2.2-2.65∶1。
摘要（英）：

This invention is a process for preparation of 2,4-heteroatom-substituted molybdena-3,3-dioxocycloalkane compounds by reacting diol-, diamino, thiol-alcohol- and amino-alcohol-compounds with the following reagents: ammonium molybdate (or in situ produced ammonium molybdate by the reaction of ammonia with molybdenum trioxide or molybdic acid) as a molybdenum source, ammonia as an additional or secondary reagent or promoter, in molar ratio NH3:Mo (amount of molybdenum in the molybdenum source) of =1:1, preferably 1-3:1, more preferably 2-3:1, and most preferred 2.2-2.65:1.

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