发明公开
EP0655092A1 IMPROVED PROCESS FOR POST-SPIN FINISHING OF POLYBENZOXAZOLE FIBERS
失效
改进的方法治疗POLYBENZOXAZOLEFASEREN SPIDER了。
- 专利标题: IMPROVED PROCESS FOR POST-SPIN FINISHING OF POLYBENZOXAZOLE FIBERS
- 专利标题(中): 改进的方法治疗POLYBENZOXAZOLEFASEREN SPIDER了。
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申请号: EP93919943.0申请日: 1993-08-09
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公开(公告)号: EP0655092A1公开(公告)日: 1995-05-31
- 发明人: ALEXANDER, Willard, E. , CHAU, Chieh-Chun , FALEY, Timothy, L.
- 申请人: THE DOW CHEMICAL COMPANY
- 申请人地址: 2030 Dow Center, Abbott Road Midland, Michigan 48640 US
- 专利权人: THE DOW CHEMICAL COMPANY
- 当前专利权人: THE DOW CHEMICAL COMPANY
- 当前专利权人地址: 2030 Dow Center, Abbott Road Midland, Michigan 48640 US
- 代理机构: Sternagel, Hans-Günther, Dr., et al
- 优先权: US19920929272 19920813
- 国际公布: WO1994004726 19940303
- 主分类号: D01F6
- IPC分类号: D01F6 ; D06M11
摘要:
Improved polybenzoxazole fibers are made by a process for finishing a spun and drawn dope fiber, which contains polybenzoxazole polymer and a solvent acid, comprising the steps of: (a) coagulating the dope fiber in an aqueous coagulant; (b) washing the coagulated fiber with an aqueous washing fluid for less than 72 hours under conditions such that the fiber contains no more than 8,000 ppm residual solvent acid (1 ppm = 1 part per million, by weight); (c) drying the fiber at a temperature of 120 °C to 300 °C until it retains no more than 2 weight percent residual moisture; and (d) heat-treating the fiber at a temperature of at least 300 °C under tension.
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