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EP0675100A2 Preparation of alpha-beta-unsaturated c3-c6 carboxylic acids 失效
Herstellung von alpha-beta-ungesättigtenC3-C6-Carbonsäuren。

Preparation of alpha-beta-unsaturated c3-c6 carboxylic acids
摘要:
The present invention provides a process for the preparation of an α,β-unsaturated C 3 -C 6 carboxylic acid of greater than 98% purity, which combines fractional distillation and melt crystallization procedures. One embodiment of the process of the invention is depicted schematically in Figure 1 wherein 1 represents a dehydrogenation reactor in which a C 3 -C 6 carboxylic acid is dehydrogenated to produce on α,β-unsaturated C 3 -C 6 carboxylic acid, 3 represents a distillation unit and 6 represents a melt crystallizer.
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