发明授权
- 专利标题: DEPOSITION OF COATINGS USING AN ATMOSPHERIC PRESSURE PLASMA JET
- 专利标题(中): 涂覆涂层用等离子束在大气压力
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申请号: EP98953847.5申请日: 1998-10-20
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公开(公告)号: EP1090159B8公开(公告)日: 2009-06-10
- 发明人: BABAYAN, Steve, E. , SELWYN, Gary, S. , HICKS, Robert, F.
- 申请人: Los Alamos National Security, LLC
- 申请人地址: Los Alamos National Laboratory LC/IP, MS A187 Los Alamos, NM 87545 US
- 专利权人: Los Alamos National Security, LLC
- 当前专利权人: Los Alamos National Security, LLC
- 当前专利权人地址: Los Alamos National Laboratory LC/IP, MS A187 Los Alamos, NM 87545 US
- 代理机构: Johnson, Richard Alan
- 优先权: US62822P 19971020
- 国际公布: WO1999020809 19990429
- 主分类号: C23C8/00
- IPC分类号: C23C8/00 ; C23C16/00 ; H05H1/24
摘要:
The use of a non-thermal source which is capable of operation at 760 torr is demonstrated. As an example of the application of the present invention, a helim/oxygen gas mixture is introduced into the annular region (20) between two coaxial electrodes (14) driven by a 13.56 MHz radio frequency (RF) source (18) at between 40 and 500 W to produce a stable plasma jet. As detected by optical emission spectroscopy (OES), a high flux of metastable oxygen and no ions are present at the exit of this plasma jet. Silicon dioxide films are deposited by introducing tetraethoxysilane (TEOS) into the effluent stream. A deposition rate of 3020 +/- 250 ANGSTROM /min. is achieved with an RF power of 400 W, 0.2 torr of TEOS, 11.1 torr of oxygen, 748.7 torr of helium, and a total gas flow rate of 41 L/m.
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