发明授权
EP1133345B1 PROCESS AND APPARATUS FOR SIZE SELECTIVE SEPARATION OF MICRO- AND NANO-PARTICLES
有权
方法和设备的微型和纳米粒子的GRÖSSSENABHÄNGIGEN分离
- 专利标题: PROCESS AND APPARATUS FOR SIZE SELECTIVE SEPARATION OF MICRO- AND NANO-PARTICLES
- 专利标题(中): 方法和设备的微型和纳米粒子的GRÖSSSENABHÄNGIGEN分离
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申请号: EP99945612.2申请日: 1999-09-09
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公开(公告)号: EP1133345B1公开(公告)日: 2010-06-16
- 发明人: SUBRAMANIAM, Bala , RAJEWSKI, Roger, A. , BOCHNIAK, David, J.
- 申请人: THE UNIVERSITY OF KANSAS
- 申请人地址: Strong Hall Lawrence, KS 66045 US
- 专利权人: THE UNIVERSITY OF KANSAS
- 当前专利权人: THE UNIVERSITY OF KANSAS
- 当前专利权人地址: Strong Hall Lawrence, KS 66045 US
- 代理机构: UEXKÜLL & STOLBERG
- 优先权: US193660 19981117
- 国际公布: WO2000029096 20000525
- 主分类号: B01D61/00
- IPC分类号: B01D61/00 ; B01D11/04 ; C30B7/00 ; C30B29/60
摘要:
Processes and apparatuses are provided for continuously harvesting particles from organic solution-laden near-critical and supercritical fluids. Broadly, the processes and apparatuses utilize a filter or separator comprising a thin membrane supported on a sintered stainless steel tube. A feed stream comprising the desired particles, a supercritical antisolvent for the particles (preferably CO2), and a solvent for the particles, is contacted with the membrane layer of the filter under supercritical conditions for the mixture of antisolvent and solvent. The preferred antisolvents are substantially miscible with the solvent and have a critical temperature of less than 160 DEG C. The desired particles are retained by the filter while the solvent and most of the antisolvent pass through the filter, resulting in separation of the particles from the solvent.
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