发明公开
- 专利标题: PROCESS FOR THE PREPARATION OF CONDENSED PHOSPHORIC ESTERS
- 专利标题(中): 制备稠凝磷酸酯的方法
-
申请号: EP99954439.8申请日: 1999-11-08
-
公开(公告)号: EP1199310A1公开(公告)日: 2002-04-24
- 发明人: NAKAMURA, Shin , NOGUCHI, Kazuo , FUJISAWA, Taku , OHKAWA, Takafumi
- 申请人: DAIHACHI CHEMICAL INDUSTRY CO., LTD.
- 申请人地址: Hiranomachi Yachiyo Bldg., 8-13, Hiranomachi 1-chome, Chuo-ku Osaka-shi, Osaka 541-0046 JP
- 专利权人: DAIHACHI CHEMICAL INDUSTRY CO., LTD.
- 当前专利权人: DAIHACHI CHEMICAL INDUSTRY CO., LTD.
- 当前专利权人地址: Hiranomachi Yachiyo Bldg., 8-13, Hiranomachi 1-chome, Chuo-ku Osaka-shi, Osaka 541-0046 JP
- 代理机构: Lucas, Brian Ronald
- 优先权: JP21275299 19990727
- 国际公布: WO0107446 20010201
- 主分类号: C07F9/12
- IPC分类号: C07F9/12 ; C08G79/04
摘要:
A condensed phosphoric ester having a very low content of isopropenyl phenyl diphenyl phosphate, which reduces heat resistance and causes the contamination of molds during the molding when the condensed phosphoric ester is used as an additive for a resin, is provided by a process including a first step of reacting a phosphorus oxytrihalide with a bisphenol A derivative at a specific ratio to prepare a phosphorohalidate; a second step of removing unreacted phosphorus oxytrihalide; a third step of reacting the reaction product obtained in the second step with a monophenol-based compound at a temperature equal to or lower than 120°C; and a fourth step of reacting the phosphorohalidate with the monophenol-based compound at a temperature equal to or higher than 120°C.
公开/授权文献
- EP1199310B1 PROCESS FOR THE PREPARATION OF CONDENSED PHOSPHORIC ESTERS 公开/授权日:2003-11-05
信息查询