发明公开
- 专利标题: VERFAHREN UND VORRICHTUNG ZUM HERSTELLEN VON DIMETHYLETHER AUS METHANOL
- 专利标题(英): Method and device for producing dimethyl ether from methanol
- 专利标题(中): 方法和设备用于生产二甲醚的甲醇
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申请号: EP09775097.0申请日: 2009-11-19
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公开(公告)号: EP2367780A1公开(公告)日: 2011-09-28
- 发明人: AHLERS, Bernd , BIRKE, Gerhard , KÖMPEL, Harald , BACH, Hermann , ROTHÄMEL, Martin , LIEBNER, Waldemar , BOII, Walter , GRONEMANN, Veronika
- 申请人: Lurgi GmbH
- 申请人地址: Lurgiallee 5 60439 Frankfurt am Main DE
- 专利权人: Lurgi GmbH
- 当前专利权人: Lurgi GmbH
- 当前专利权人地址: Lurgiallee 5 60439 Frankfurt am Main DE
- 优先权: DE102008058931 20081125
- 国际公布: WO2010060566 20100603
- 主分类号: C07C41/09
- IPC分类号: C07C41/09 ; C07C43/04 ; B01D3/14
摘要:
A process produces dimethyl ether (DME) from methanol (MeOH). The process includes charging a feed mixture consisting of raw MeOH and a process-internally obtained return flow substantially consisting of unconverted MeOH and reaction water to an MeOH column. The feed mixture is evaporated in the MeOH column to form a first distillate substantially consisting of vaporous MeOH. The first distillate is supplied to a reactor and the MeOH is converted to DME by splitting off water in the reactor so as to form a reaction mixture. The reaction mixture is withdrawn from the reactor, charged to a mixture column and separated into a bottom product substantially consisting of water and a second distillate substantially consisting of DME and MeOH. The second distillate is separated in a DME column into a third distillate substantially consisting of DME, a bottom product consisting essentially of water-poor MeOH, and uncondensable gases discharged overhead. The bottom product is either supplied to a top of the MeOH column or mixed with another bottom product withdrawn from a forerun column.
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