发明公开
- 专利标题: DEVICE AND METHOD FOR CRYSTALLIZING (METH)ACRYLIC ACID
- 专利标题(中): 装置和方法结晶(甲基)丙烯酸
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申请号: EP10794063申请日: 2010-06-24
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公开(公告)号: EP2450340A4公开(公告)日: 2015-08-05
- 发明人: SAKAMOTO KAZUHIKO , UENO KOJI , ISHII YOSHITAKE , KITAURA MASATSUGU
- 申请人: NIPPON CATALYTIC CHEM IND
- 专利权人: NIPPON CATALYTIC CHEM IND
- 当前专利权人: NIPPON CATALYTIC CHEM IND
- 优先权: JP2009158971 2009-07-03
- 主分类号: C07C51/43
- IPC分类号: C07C51/43 ; B01D9/00 ; B01D9/02 ; C07C57/07
摘要:
The objective of the present invention is to provide a crystallization device and a crystallization process for obtaining (meth) acrylic acid with higher purity without causing leakage of a crude solution by preventing complete clogging in a crystallization tube from occurring. The device for crystallizing (meth)acrylic acid according to the present invention is characterized in comprising a crude (meth)acrylic acid solution supply part, a crystallization tube, a heat medium supply tube, a heat medium discharge tube, a storage part of a crude (meth)acrylic acid solution passed through the crystallization tube, a tube for circulating and supplying the crude (meth)acrylic acid solution to the supply part from the storage part, and a pump for circulating and supplying the crude (meth) acrylic acid solution to the supply part from the storage part; and further comprising a pressure meter in the circulate-supply tube; wherein the device is used for carrying out dynamic crystallization in a batch manner by circulating the crude (meth)acrylic acid solution to flow the crude solution downward along the inner wall of the crystallization tube in a coating film-like state.
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