发明公开
EP2518489A1 METHOD FOR COLLECTING SAMPLE AND DEVICE FOR COLLECTING SAME
审中-公开
VERFAHREN ZUR ENTNAHME EINER PROBE UND VORRICHTUNG ZU DEREN ENTNAHME
- 专利标题: METHOD FOR COLLECTING SAMPLE AND DEVICE FOR COLLECTING SAME
- 专利标题(中): VERFAHREN ZUR ENTNAHME EINER PROBE UND VORRICHTUNG ZU DEREN ENTNAHME
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申请号: EP10845684.9申请日: 2010-02-12
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公开(公告)号: EP2518489A1公开(公告)日: 2012-10-31
- 发明人: SOTOMARU, Katsuhiko , ZHOU, Xiao-jing , YAMASAKI, Kazuhiko , SATO, Atsushi
- 申请人: GL Sciences Incorporated
- 申请人地址: 6-22-1, Nishi-shinjuku Shinjuku-ku Tokyo 163-1130 JP
- 专利权人: GL Sciences Incorporated
- 当前专利权人: GL Sciences Incorporated
- 当前专利权人地址: 6-22-1, Nishi-shinjuku Shinjuku-ku Tokyo 163-1130 JP
- 代理机构: Schmid, Wolfgang
- 国际公布: WO2011099079 20110818
- 主分类号: G01N30/08
- IPC分类号: G01N30/08 ; G01N30/00 ; G01N30/04
摘要:
An object of the present invention is to provide a sample trapping method and a sample trapping apparatus. The present invention is suitable, for example, for analysis by a gas chromatograph-mass spectrometer. A sample is not cooled by a refrigerant such as liquid nitrogen in the present invention. Instead, a cold storage refrigerator such as a Stirling refrigerator or a Gifford-McMahon refrigerator is used. As a result, the operability is improved and the running cost is reduced. In addition, a refrigerant pipe is not used in the present invention. It is thus possible to reduce the size and weight of the apparatus, to improve the efficiency and accuracy for cooling the sample, and to rapidly cool the sample. Furthermore, it is possible to rapidly heat the sample. As a result, the trapped sample is instantaneously desorbed. Therefore, the present invention makes it possible to achieve cryofocusing in gas chromatography (particularly in high-speed gas chromatography).
Solutions of the present invention include a sample trapping method using a sample conduit for trapping a gas sample by cooling or desorbing the gas sample by heating. The solutions further include cooling a sample conduit (17) by arranging the sample conduit (17) in the vicinity of, or bringing the sample conduit (17) into contact with, a cooling part of a cooling device (20) based on a cold storage refrigerator.
Solutions of the present invention include a sample trapping method using a sample conduit for trapping a gas sample by cooling or desorbing the gas sample by heating. The solutions further include cooling a sample conduit (17) by arranging the sample conduit (17) in the vicinity of, or bringing the sample conduit (17) into contact with, a cooling part of a cooling device (20) based on a cold storage refrigerator.
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