发明公开
- 专利标题: PROCESS FOR PREPARING CHOLINE HYDROXIDE FROM TRIMETHYLAMINE AND ETHYLENE OXIDE
- 专利标题(中): 用于生产三甲胺和乙烯胆碱
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申请号: EP13738032申请日: 2013-01-17
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公开(公告)号: EP2804477A4公开(公告)日: 2015-09-23
- 发明人: LI RUOKANG , DIXIT RAVINDRA S , PATEL AVANI M , CHEN XIAOYUN , PELL RANDY J , PENDERGAST JOHN G
- 申请人: DOW AGROSCIENCES LLC
- 专利权人: DOW AGROSCIENCES LLC
- 当前专利权人: DOW AGROSCIENCES LLC
- 优先权: US201261588234 2012-01-19; US201261720711 2012-10-31
- 主分类号: A01N33/12
- IPC分类号: A01N33/12 ; C07C213/04 ; C07C215/40 ; C07C217/08
摘要:
Processes for preparing N,N,N-trimethylethanolammonium hydroxide (choline hydroxide) and the choline hydroxide produced are described. These processes minimize the production of byproduct mono-ethoxylated and di-ethyoxylated choline in the product choline hydroxide. The processes generally include feeding ethylene oxide, trimethylamine, and water into a first reactor to create a first reactor product under temperature controlled conditions. The product of the first reactor is fed into a second reactor to form a second reactor product under uncontrolled, adiabatic, conditions. Finally, any unreacted trimethylamine in the second reactor product is removed to form a final product comprising choline hydroxide. Additional reactors can be used for the ethylene oxide and trimethylamine reaction.
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