发明公开
- 专利标题: METHOD FOR PRODUCING DIFLUOROPHOSPHATE
- 专利标题(中): VERFAHREN ZUR HERSTELLUNG VON DIFLUORPHOSPHAT
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申请号: EP14808166.4申请日: 2014-06-06
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公开(公告)号: EP2939978A1公开(公告)日: 2015-11-04
- 发明人: YAHATA Naoki , NISHIDA Tetsuo , MINAMIGAWA Shuichi
- 申请人: Stella Chemifa Corporation
- 申请人地址: 3-6-3, Awaji-machi Chuo-ku Osaka 541-0047 JP
- 专利权人: Stella Chemifa Corporation
- 当前专利权人: Stella Chemifa Corporation
- 当前专利权人地址: 3-6-3, Awaji-machi Chuo-ku Osaka 541-0047 JP
- 代理机构: Sajda, Wolf E.
- 优先权: JP2013121328 20130607
- 国际公布: WO2014196627 20141211
- 主分类号: C01B25/455
- IPC分类号: C01B25/455 ; H01G11/62 ; H01M10/0567 ; H01M10/0568
摘要:
Provided is a method for producing a difluorophosphate, which can easily and industrially advantageously produce a high-purity difluorophosphate . The method includes a step of producing a difluorophosphate in the fluorophosphoric acid solution by reacting hydrofluoric acid anhydride containing no solvent with an oxoacid and/or the like of phosphorous to produce a fluorophosphoric acid solution; a step of adding a hexafluorophosphate to the fluorophosphoric acid solution in the absence of respective halides, carbonates, borates, phosphates, hydroxides, and oxides of an alkali metal and the like; and a step of heating and drying the fluorophosphoric acid solution containing the difluorophosphate to distill away a fluorophosphoric acid, or a step of depositing the difluorophosphate in the fluorophosphoric acid solution by crystallization, subsequently separating the difluorophosphate by solid-liquid separation, and distilling away a fluorophosphoric acid contained in the difluorophosphate after the solid-liquid separation.
公开/授权文献
- EP2939978B1 METHOD FOR PRODUCING DIFLUOROPHOSPHATE 公开/授权日:2017-08-16
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