- 专利标题: Garnet powder, manufacturing method thereof, solid electrolyte sheet using hot press and manufacturing method thereof
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申请号: US14716491申请日: 2015-05-19
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公开(公告)号: US10008740B2公开(公告)日: 2018-06-26
- 发明人: Ju Young Sung , Ho Taek Lee , Eun Ji Kwon , Yong Jun Jang , Ji Na Kim
- 申请人: HYUNDAI MOTOR COMPANY
- 申请人地址: KR Seoul
- 专利权人: HYUNDAI MOTOR COMPANY
- 当前专利权人: HYUNDAI MOTOR COMPANY
- 当前专利权人地址: KR Seoul
- 代理机构: McDermott Will & Emery LLP
- 优先权: KR10-2014-0106858 20140818
- 主分类号: H01M10/00
- IPC分类号: H01M10/00 ; H01M10/0562 ; H01M10/0525 ; C01B33/26
摘要:
The present disclosure relates to garnet powder, a manufacturing method thereof, a solid electrolyte sheet using a hot press, and a manufacturing method thereof. In particular, the present disclosure provides a method for manufacturing Li7La3Zr2O12 (LLZ) garnet powder including preparing a mixture by first dry mixing Li2CO3, La2O3, ZrO2, and Al2O3. The mixture is first calcinated for 5 to 7 hours in a temperature range of 800 to 1000° C. The calcinated mixture is ground to a powder with an average particle size of 1 to 4 μm through dry grinding. A cubic-phased LLZ garnet powder is prepared by second calcinating the ground mixture for 10 to 30 hours in a temperature range of 1100 to 1300° C.
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