Invention Grant
- Patent Title: Method for producing acetic acid
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Application No.: US15540177Application Date: 2017-05-25
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Publication No.: US10266473B2Publication Date: 2019-04-23
- Inventor: Masahiko Shimizu
- Applicant: DAICEL CORPORATION
- Applicant Address: JP Osaka-Shi, Osaka
- Assignee: DAICEL CORPORATION
- Current Assignee: DAICEL CORPORATION
- Current Assignee Address: JP Osaka-Shi, Osaka
- Agency: Birch, Stewart, Kolasch & Birch, LLP
- Priority: JP2016-211922 20161028; JP2017-039388 20170302
- International Application: PCT/JP2017/019572 WO 20170525
- International Announcement: WO2018/078924 WO 20180503
- Main IPC: C07C51/12
- IPC: C07C51/12 ; C07C51/44 ; B01D1/30 ; B01D53/14 ; B01D3/14

Abstract:
Provided is a method for producing acetic acid, which suppresses catalyst precipitation and accumulation in an evaporator, can efficiently recycle catalysts to a reaction vessel, and can contribute to maintenance and improvement in acetic acid productivity and securing of safety operation. In the method, the evaporator has a catalyst precipitation and accumulation prevention structure: (a) structure where inclination angle θ of inside wall surface of an inverted truncated conical cylindrical connection portion is 5° to 85°; and/or (b) structure where a vortex breaker comprising a plate-like vortex breaker main body and a leg is disposed such that the vortex breaker main body covers right above the connection portion of an evaporator bottom part to a residual liquid stream recycle line, and linear velocity r of the residual liquid stream passing through a gap between the vortex breaker main body and the evaporator bottom part is larger than 10 m/h.
Public/Granted literature
- US20180118649A1 METHOD FOR PRODUCING ACETIC ACID Public/Granted day:2018-05-03
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