Invention Grant
- Patent Title: Microcapsules and macrocapsules having low remnant free formaldehyde microcapsules and methods of making same
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Application No.: US15991839Application Date: 2018-05-29
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Publication No.: US10287470B2Publication Date: 2019-05-14
- Inventor: Carl M. Lentz , David R. Virgallito , Jerry K. Lawson
- Applicant: MICROTEK LABORATORIES, INC.
- Applicant Address: US OH Dayton
- Assignee: Microtek Laboratories, INC.
- Current Assignee: Microtek Laboratories, INC.
- Current Assignee Address: US OH Dayton
- Agency: FisherBroyles, LLP
- Agent Susan M. Oiler
- Main IPC: B01J13/14
- IPC: B01J13/14 ; C09K5/06 ; F28D20/02 ; B01J13/18 ; C08G12/32

Abstract:
A microcapsule or microcapsule having a polymer wall comprising a melamine formaldehyde reacted with a crosslinking agent to form a unit cell according to a general formula (II) and/or the polymer wall has a FT-IR Spectrum as shown in FIG. 4. The crosslinking agent is a mixture of a reaction product of a cyclic urea (U) and a multifunctional aldehyde (A), and at least one crosslinker selected from the following group: a reaction products of (i) an aminotriazine and at least one aldehyde selected from the group consisting of aliphatic monoaldehydes and multifunctional aliphatic aldehydes, (ii) urea and/or cyclic ureas and formaldehyde, or (iii) phenols and aliphatic monoaldehydes, or from alkoxycarbonylaminotriazines, or multifunctional isocyanates, epoxides, aziridines, and carbodiimides.
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