Invention Grant
- Patent Title: Aqueous colorimetric fluoride detection
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Application No.: US15951927Application Date: 2018-04-12
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Publication No.: US10794882B2Publication Date: 2020-10-06
- Inventor: Darren Kent MacFarland , Angella Nicholle Greenawalt
- Applicant: Hach Company
- Applicant Address: US CO Loveland
- Assignee: HACH COMPANY
- Current Assignee: HACH COMPANY
- Current Assignee Address: US CO Loveland
- Agency: Ference & Associates LLC
- Main IPC: G01N31/22
- IPC: G01N31/22 ; G01N33/18 ; G01N21/78

Abstract:
An embodiment provides a method for measuring fluoride concentration in an aqueous solution, including: preparing a polyethylene glycol (PEG) monomethyl ether to produce an ester; reacting the ester in the presence of ammoniated tetrahydrofuran to produce an amino polyethylene glycol; placing, in a solution comprising a benzaldehyde species with a phenol functional group and a carboxylic acid functional group, a 2,3,3-trimethylindolenine derivative to produce a hemicyanine with a phenol functional group and a carboxylic acid functional group; combining, in a polar aprotic solvent, the hemicyanine with the phenol functional group and carboxylic acid functional group with a 1,1-carbonyldiimidazole (CDI) and adding the amino-PEG to produce a hemicyanine-PEG; and creating a fluoride sensitive hemicyanine species by reacting the hemicyanine-PEG that contains a phenol functional group with a SiR3 species. Other embodiments are described and claimed.
Public/Granted literature
- US20190317064A1 AQUEOUS COLORIMETRIC FLUORIDE DETECTION Public/Granted day:2019-10-17
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