Invention Grant
- Patent Title: Production of pulverulent, porous crystalline metal silicates by means of flame spray pyrolysis
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Application No.: US16770593Application Date: 2018-11-23
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Publication No.: US11192794B2Publication Date: 2021-12-07
- Inventor: Franz Schmidt , Johan Anton , Matthias Pascaly , Andrea Heinroth , Stefan Wieland , Heiko Morell , Peter Kress , Michael Hagemann
- Applicant: EVONIK OPERATIONS GMBH
- Applicant Address: DE Essen
- Assignee: EVONIK OPERATIONS GMBH
- Current Assignee: EVONIK OPERATIONS GMBH
- Current Assignee Address: DE Essen
- Agency: Law Office of: Michael A. Sanzo, LLC
- Priority: DE17205799.4 20171207
- International Application: PCT/EP2018/082304 WO 20181123
- International Announcement: WO2019/110322 WO 20190613
- Main IPC: C01B39/02
- IPC: C01B39/02 ; C01B33/20 ; C01B39/20 ; C01B39/46 ; C01B39/14 ; C01B39/26 ; C01B39/38

Abstract:
The present invention relates to a process for preparing a pulverulent, porous crystalline metal silicate, comprising the following steps: a) hydrothermal synthesis in an aqueous mixture comprising (A) at least one silicon source, (B) at least one metal source and (C) at least one mineralizer to obtain an aqueous suspension comprising a porous crystalline metal silicate as reaction product; and b) calcination of the reaction product, characterized in that the calcination is conducted by means of flame spray pyrolysis at an adiabatic combustion temperature within a range of 450-2200° C., wherein the suspension having a solids content of 70% by weight which is obtained in step a) is sprayed into a flame generated by combustion of a fuel in the presence of oxygen to form a pulverulent, porous crystalline metal silicate.
Public/Granted literature
- US20210163304A1 PRODUCTION OF PULVERULENT, POROUS CRYSTALLINE METAL SILICATES BY MEANS OF FLAME SPRAY PYROLYSIS Public/Granted day:2021-06-03
Information query
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