Invention Grant
- Patent Title: Process for preparing 2-exo-(2-Methylbenzyloxy)-1-methyl-4-isopropyl-7-oxabicyclo[2.2.1]heptane
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Application No.: US16498625Application Date: 2018-03-23
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Publication No.: US11384093B2Publication Date: 2022-07-12
- Inventor: Stefan Benson , Michael Rack , Christiane Alznauer , Roland Goetz , Bernd Wolf
- Applicant: BASF Agro B.V.
- Applicant Address: NL Amhem
- Assignee: BASF Agro B.V.
- Current Assignee: BASF Agro B.V.
- Current Assignee Address: NL Amhem
- Agency: Marshall, Gerstein & Borun LLP
- Priority: EP17164278 20170331
- International Application: PCT/EP2018/057397 WO 20180323
- International Announcement: WO2018/177907 WO 20181004
- Main IPC: C07D493/08
- IPC: C07D493/08 ; A01N25/02 ; A01N43/90
![Process for preparing 2-exo-(2-Methylbenzyloxy)-1-methyl-4-isopropyl-7-oxabicyclo[2.2.1]heptane](/abs-image/US/2022/07/12/US11384093B2/abs.jpg.150x150.jpg)
Abstract:
This invention relates to a process for preparing (±)-2-exo-(2-Methylbenzyloxy)-1-methyl-4-iso-propyl-7-oxabicyclo[2.2.1]heptane of the formula (I) any of its individual enantiomers or any non-racemic mixture thereof, comprising the step of reacting (±)-2-exo-hydroxy-1-methyl-4-isopropyl-7-oxabicyclo[2.2.1]heptane of the formula (II) any of its individual enantiomers or any non-racemic mixture thereof with a 2-Methylbenzyl compound of the formula (III) wherein X is a leaving group, in the presence of at least one base, at least one catalyst selected from rubidium salts, cesium salts and any combination thereof and at least one inert organic solvent S1.
Public/Granted literature
- US20200031842A1 PROCESS FOR PREPARING 2-EXO-(2-METHYLBENZYLOXY)-1-METHYL-4-ISOPROPYL-7-OXABICYCLO[2.2.1]HEPTANE Public/Granted day:2020-01-30
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