- 专利标题: Hydroxypropyl methyl cellulose phthalate and method for producing the same
-
申请号: US17083617申请日: 2020-10-29
-
公开(公告)号: US11873351B2公开(公告)日: 2024-01-16
- 发明人: Taishi Kitaguchi , Junichi Matsubara , Mitsuhiro Yoshida
- 申请人: Shin-Etsu Chemical Co., Ltd.
- 申请人地址: JP Tokyo
- 专利权人: Shin-Etsu Chemical Co., Ltd.
- 当前专利权人: Shin-Etsu Chemical Co., Ltd.
- 当前专利权人地址: JP Tokyo
- 代理机构: Myers Bigel, P.A.
- 优先权: JP 19200047 2019.11.01
- 主分类号: C08B3/16
- IPC分类号: C08B3/16 ; C08B13/00
摘要:
There is provided a method for producing hydroxypropyl methyl cellulose phthalate (HPMCP), including an esterification step of reacting hydroxypropyl methyl cellulose with a carboxybenzoylating agent in the presence of an aliphatic carboxylic acid in a kneader reactor equipped with two or more stirring blades rotating around their own axes and orbitally revolving, to obtain a reaction product solution containing HPMCP; a precipitation step of precipitating the HPMCP by mixing the reaction product solution with water to obtain a suspension of the precipitated HPMCP; and a washing and recovery step of washing the HPMCP in the suspension and recovering the washed HPMCP. Further, there is provided HPMCP having yellowness at 20° C. of 10.0 or less, as determined in a 10% by mass solution of the HPMCP in acetone.
公开/授权文献
信息查询