- 专利标题: Energy-saving method for preparing electronic-grade carbonate
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申请号: US18254846申请日: 2022-10-11
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公开(公告)号: US12037316B2公开(公告)日: 2024-07-16
- 发明人: Hongxing Wang , Haiyong Li , Guangqiang Zheng , Fei Li
- 申请人: TIANJIN UNIVERSITY OF SCIENCE & TECHNOLOGY
- 申请人地址: CN Tianjin
- 专利权人: TIANJIN UNIVERSITY OF SCIENCE & TECHNOLOGY
- 当前专利权人: TIANJIN UNIVERSITY OF SCIENCE & TECHNOLOGY
- 当前专利权人地址: CN Tianjin
- 代理机构: Getech Law LLC
- 代理商 Jun Ye
- 国际申请: PCT/CN2022/124504 2022.10.11
- 国际公布: WO2023/178991A 2023.09.28
- 进入国家日期: 2023-05-26
- 主分类号: C07C68/08
- IPC分类号: C07C68/08 ; C07C68/06
摘要:
The present disclosure discloses an energy-saving method for preparing electronic-grade carbonate, including the following steps that: industrial-grade dimethyl carbonate and anhydrous ethanol enter a reaction process after being preheated by a preheater, and are subjected to an esterification reaction under the action of a catalyst to obtain a mixture containing dimethyl carbonate, ethyl methyl carbonate and diethyl carbonate, and an azeotrope of dimethyl carbonate and methanol; the above-mentioned mixture enters a recovery process of dimethyl carbonate to recover unreacted dimethyl carbonate; a mixture of ethyl methyl carbonate and diethyl carbonate then enters a crude separation process to obtain crude ethyl methyl carbonate and crude diethyl carbonate; and the crude ethyl methyl carbonate is subjected to a refining process of ethyl methyl carbonate to obtain electronic-grade ethyl methyl carbonate, and the crude diethyl carbonate is subjected to a refining process of diethyl carbonate to obtain electronic-grade diethyl carbonate.
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