Invention Grant
- Patent Title: Continuous production method of diester-based material
-
Application No.: US17603208Application Date: 2020-07-02
-
Publication No.: US12084413B2Publication Date: 2024-09-10
- Inventor: Jae Hun Jeong , Sung Kyu Lee , Yeon Uk Choo , Hyun Kyu Kim , Seok Goo Lee
- Applicant: LG CHEM, LTD.
- Applicant Address: KR Seoul
- Assignee: LG Chem, Ltd.
- Current Assignee: LG Chem, Ltd.
- Current Assignee Address: KR Seoul
- Agency: Bryan Cave Leighton Paisner LLP
- Priority: KR 20190080460 2019.07.04
- International Application: PCT/KR2020/008660 2020.07.02
- International Announcement: WO2021/002700A 2021.01.07
- Date entered country: 2021-10-12
- Main IPC: C07C67/08
- IPC: C07C67/08 ; B01J19/00 ; C07C67/52 ; C07C69/75 ; C07C69/80 ; C07C69/82

Abstract:
The present disclosure relates to a continuous production method of a diester-based material in a continuous production process comprising a reaction part in which a total of N reaction units from a first reaction unit to an N-th reaction unit are connected in series. The method comprising the step of feeding dicarboxylic acid and a primary alcohol, wherein the feed of the primary alcohol is divided into front-end feed of being fed into a first reaction unit and rear-end feed of being fed into one or more reaction units selected among from a second reaction unit to an N-th reaction unit, wherein the amount of the rear-end feed is 5 to 80 wt % based on the total feed amount of the primary alcohol into a reaction part, and the N is an integer of 3 to 6. According to the present invention, it is possible to ensure the ease of process operation through reducing the amount of reflux compared to a typical batch process and reducing the volume of steam for heating a reactor, and to ensure the economic feasibility of a product through saving energy.
Public/Granted literature
- US20220185761A1 CONTINUOUS PRODUCTION METHOD OF DIESTER-BASED MATERIAL Public/Granted day:2022-06-16
Information query