发明申请
- 专利标题: Process for production of bisphenol a
- 专利标题(中): 生产双酚A的方法
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申请号: US10508012申请日: 2003-03-19
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公开(公告)号: US20050222467A1公开(公告)日: 2005-10-06
- 发明人: Masahiro Kodama , Kazuyuki Hirano , Norio Ogata
- 申请人: Masahiro Kodama , Kazuyuki Hirano , Norio Ogata
- 优先权: JP2002-96701 20020329
- 国际申请: PCT/JP03/03330 WO 20030319
- 主分类号: C07C37/84
- IPC分类号: C07C37/84 ; C07C39/16
摘要:
In the process for producing bisphenol A comprising crystallizing an adduct of bisphenol A and phenol from a phenol solution of bisphenol A obtained by reacting phenol and acetone in the presence of an acid catalyst, treating the formed slurry by solid-liquid separation and removing phenol from the solid component, a layer of the crystalline adduct is formed on a filter by filtering slurry (1) comprising the crystalline adduct, washing the layer of the adduct with a washing liquid, dissolving the layer of the adduct in a solution comprising phenol, producing slurry (2) comprising the crystalline adduct by crystallization, and separating the crystalline adduct by centrifugation of slurry (2). When bisphenol A is separated from the reaction mixture, the adduct of bisphenol A and phenol can be recovered from the mother liquor of the reaction efficiently at a high purity in accordance with the above process.
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