Invention Application
- Patent Title: Process for preparing caprolactam by beckmann rearrangement
- Patent Title (中): 贝克曼重排制备己内酰胺的方法
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Application No.: US10557771Application Date: 2004-05-17
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Publication No.: US20070083043A1Publication Date: 2007-04-12
- Inventor: Petrus Jozef Thomissen , Joannes Albertus Lemmens , Theodorus Smeets
- Applicant: Petrus Jozef Thomissen , Joannes Albertus Lemmens , Theodorus Smeets
- Priority: EP03076590/3 20030523; EP03076591.1 20030523; EP03076589.5 20030523; EP03076592.9 20030523
- International Application: PCT/EP04/05340 WO 20040517
- Main IPC: C07D201/04
- IPC: C07D201/04

Abstract:
The invention relates to a process for preparing caprolactam by Beckmann rearrangement of cyclohexanone oxime by feeding cyclohexanone oxime to a reaction mixture comprising (i) sulfuric acid (ii) S03 and (iii) caprolactam, wherein the S03 content of the reaction mixture is between 9 and 20 wt. % and the molar ratio M of the reaction mixture defined as (nSO3+nH2SO4)/ncap is between 1 and 1.4, wherein nSO3=quantity of SO3 in reaction mixture, in mol nH2SO4=quantity of H2SO4 in reaction mixture, in mol ncap=quantity of caprolactam in reaction mixture, in mol.
Public/Granted literature
- US07351820B2 Process for preparing caprolactam by Beckmann rearrangement Public/Granted day:2008-04-01
Information query