发明申请
- 专利标题: Process for producing adamantane
- 专利标题(中): 生产金刚烷的方法
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申请号: US10590995申请日: 2005-02-28
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公开(公告)号: US20070173678A1公开(公告)日: 2007-07-26
- 发明人: Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito , Toshiaki Kusaba
- 申请人: Jun Mase , Shinji Miyamoto , Akio Kojima , Masao Saito , Toshiaki Kusaba
- 申请人地址: JP Chiyoda-ku 100-8321
- 专利权人: Idemitsu Kosan Co., Ltd
- 当前专利权人: Idemitsu Kosan Co., Ltd
- 当前专利权人地址: JP Chiyoda-ku 100-8321
- 优先权: JP2004-056395 20040301
- 国际申请: PCT/JP05/03288 WO 20050228
- 主分类号: C07C5/13
- IPC分类号: C07C5/13
摘要:
An industrially advantageous process for producing adamantane by which high-purity adamantane reduced in coloration is efficiently produced while minimizing the loss. The process, which is for producing adamantane by isomerizing trimethylenenorbornane, includes (A) a reaction step of isomerizing the starting material, (B) a concentration step of concentrating the adamantane contained in the resultant liquid reaction mixture, (C) a crystallization step of precipitating the concentrated adamantane, (D) a solid-liquid separation step of separating the adamantane crystals from the slurry resulting from the crystallization, (E) a washing step of washing the isolated adamantane crystals, and (F) a drying step of drying the adamantane crystals washed, characterized in that the mass ratio of the endo-trimethylenenorbornane to the adamantane each contained in the materials to be subjected to the crystallization step (C) (endo-trimethylenenorbornane/adamantane) is 0.25 or lower.
公开/授权文献
- US07381855B2 Process for producing adamantane 公开/授权日:2008-06-03