发明申请
- 专利标题: Sample Tube for Solid-State Nuclear Magnetic Resonance Apparatus Magic Angle High-Speed Rotation Method and Method for Measuring Nuclear Magnetic Resonance Absorption Spectrum Employing It
- 专利标题(中): 用于固态核磁共振装置的样品管魔角高速旋转方法和测量使用它的核磁共振吸收谱的方法
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申请号: US11791543申请日: 2005-04-15
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公开(公告)号: US20080007262A1公开(公告)日: 2008-01-10
- 发明人: Kazuo Yamauchi , Tetsuo Asakura
- 申请人: Kazuo Yamauchi , Tetsuo Asakura
- 专利权人: Kirin Beer Kabushiki Kaisha
- 当前专利权人: Kirin Beer Kabushiki Kaisha
- 优先权: JP2004-017603 20041126
- 国际申请: PCT/JP05/07303 WO 20050415
- 主分类号: G01R33/30
- IPC分类号: G01R33/30 ; G01R33/44
摘要:
The present invention discloses a sample tube for the magic angle high-speed rotation method used in a solid nuclear magnetic resonance device probe wherein a radio wave irradiation/detection coil is disposed close to a sample and a method of measuring a high resolution nuclear magnetic resonance absorption spectrum using the same. This tube is suitable for solid nuclear magnetic resonance (solid NMR) measurements of minute amounts of sample. The sample tube has a capillary part filled with a sample and non-capillary parts situated at its two ends, and a spinner which can be detachably inserted into at least one of the outer ends of the non-capillary parts. The capillary part and non-capillary parts are made of a ceramic and/or polymer material.