- 专利标题: Method of preparing metallic nanoparticles and materials thus obtained
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申请号: US12802970申请日: 2010-06-17
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公开(公告)号: US20100261005A1公开(公告)日: 2010-10-14
- 发明人: Julio Santarén Romé , Francisco Javier Limpo Orozco , Eduardo Aguilar Díez , Antonio Álvarez Berenguer , José Moya Corral , Carlos Pecharroman Garcia
- 申请人: Julio Santarén Romé , Francisco Javier Limpo Orozco , Eduardo Aguilar Díez , Antonio Álvarez Berenguer , José Moya Corral , Carlos Pecharroman Garcia
- 专利权人: TOLSA, S.A.
- 当前专利权人: TOLSA, S.A.
- 优先权: ESP200302396 20031015
- 主分类号: B32B5/16
- IPC分类号: B32B5/16 ; B01J21/16 ; B01J23/40 ; B01J23/70
摘要:
The invention relates to a method of preparing metallic nanoparticles and to the materials thus obtained. More specifically, the invention relates to a method of preparing metallic nanoparticles consisting in: selecting a precursor from the salts, hydroxides and oxides of metallic elements that can be reduced at temperatures below the clay silicate network destruction temperature; and depositing said precursor on a support selected from pseudolaminar phyllosilicate clays. According to the invention the method comprises: (i) a deposition step in which the precursor is deposited on the support: (ii) when the precursor is selected from among salts and hydroxides, a thermal decomposition step in a controlled atmosphere, in which the precursor is subjected to a decomposition process and is transformed into an oxide of the metallic element: and (iii) a reduction step in which the oxide of the metallic element is subjected to a reduction process in a controlled atmosphere. The aforementioned method is performed at temperatures below the clay silicate network destruction temperature.
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