发明申请
- 专利标题: PROCESS FOR THE PRODUCTION OF ISOCYANATES
- 专利标题(中): 生产异氰酸酯的方法
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申请号: US12851604申请日: 2010-08-06
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公开(公告)号: US20100298596A1公开(公告)日: 2010-11-25
- 发明人: Berthold Keggenhoff , Heinrich Lokum , Matthias Böhm
- 申请人: Berthold Keggenhoff , Heinrich Lokum , Matthias Böhm
- 申请人地址: DE Leverkusen
- 专利权人: Bayer MaterialScience AG
- 当前专利权人: Bayer MaterialScience AG
- 当前专利权人地址: DE Leverkusen
- 优先权: DE102006022448.5 20060513
- 主分类号: C07C263/10
- IPC分类号: C07C263/10
摘要:
Isocyanates, preferably diisocyanates and polyisocyanates of the diphenylmethane series (MDI), are produced by reaction of amines dissolved in a solvent with phosgene in the same solvent to form the corresponding isocyanates. Hydrogen chloride and excess phosgene are subsequently removed from the reaction mixture to obtain a crude isocyanate-containing solution. Subsequently, the crude isocyanate-containing solution is separated by distillation into isocyanates and solvent. The solvent is recycled and used for the production of solutions of the amines and of phosgene. The solvent being recycled is treated to reduce the phosgene and diisocyanate contents before being used for the production of the solution of the amine.
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