Invention Application
US20140315079A1 METHOD FOR PREPARING PENTACYCLIC ANION SALT 审中-公开
制备PENTACYCLIC阴离子盐的方法

  • Patent Title: METHOD FOR PREPARING PENTACYCLIC ANION SALT
  • Patent Title (中): 制备PENTACYCLIC阴离子盐的方法
  • Application No.: US14357784
    Application Date: 2012-10-29
  • Publication No.: US20140315079A1
    Publication Date: 2014-10-23
  • Inventor: Gregory SchmidtMiguel Flasque
  • Applicant: ARKEMA FRANCE
  • Priority: FR1160301 20111114
  • International Application: PCT/FR2012/052489 WO 20121029
  • Main IPC: H01M10/0568
  • IPC: H01M10/0568
METHOD FOR PREPARING PENTACYCLIC ANION SALT
Abstract:
A method for preparing an imidazole compound with the following formula: wherein Rf is a fluorinated alkyl group comprising between 1 and 5 carbon atoms, said method including: (a) the reaction of the diaminomaleonitrile with the following formula: with the compound with the following formula: wherein Y represents a chlorine atom or the OCORf group to form the salified amide compound with the following formula: at temperature T1, and (b) the dehydration of the salified amide compound with formula (IVa) and/or the corresponding amino (IVb) to form the imidazole compound with formula (III), at temperature T2 higher than T1.
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