Invention Application
US20150079692A1 METHOD OF DETERMINING PHENOXY HERBICIDES IN WATER SAMPLES BY PHASE TRANSFER MICROEXTRACTION WITH SIMULTANEOUS DERIVATIZATION AND GAS-CHROMATOGRAPHY MASS-SPECTROMETRY ANALYSIS 有权
通过相转移微萃取同时衍生化和气相色谱质谱分析法测定水样中苯酚类除草剂的方法

METHOD OF DETERMINING PHENOXY HERBICIDES IN WATER SAMPLES BY PHASE TRANSFER MICROEXTRACTION WITH SIMULTANEOUS DERIVATIZATION AND GAS-CHROMATOGRAPHY MASS-SPECTROMETRY ANALYSIS
Abstract:
A method for determining the concentration of a phenoxy herbicide in an aqueous sample, by simultaneously phase-transfer catalyst extracting and alkylating an aqueous sample comprising a phenoxy herbicide to form a sample composition, and measuring an amount of the alkylated phenoxy herbicide in the sample composition. The method includes controlling factors such as pH of the aqueous matrix, temperature, extraction duration, type and amount of derivation reagents, and type and amount of phase transfer catalyst.
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