Invention Application
US20160083318A1 PROCESS FOR THE PREPARATION OF GLYCOLS 有权
制备甘油的方法

  • Patent Title: PROCESS FOR THE PREPARATION OF GLYCOLS
  • Patent Title (中): 制备甘油的方法
  • Application No.: US14781756
    Application Date: 2014-04-01
  • Publication No.: US20160083318A1
    Publication Date: 2016-03-24
  • Inventor: Evert VAN DER HEIDEGovinda Subbanna WAGLE
  • Applicant: SHELL OIL COMPANY
  • Priority: EP13162503.0 20130405
  • International Application: PCT/EP2014/056524 WO 20140401
  • Main IPC: C07C29/132
  • IPC: C07C29/132
PROCESS FOR THE PREPARATION OF GLYCOLS
Abstract:
The invention provides a process for the preparation of ethylene glycol and 1,2-propylene glycol from starting material comprising one or more saccharides, by contacting said starting material with hydrogen in a reactor in the presence of a solvent and a catalyst system with catalytic hydrogenation abilities, wherein the process comprises the steps of: i) introducing a first portion of the starting material into the reactor such that the initial concentration of the saccharide in the solvent in the reactor is no more than 2 wt %; ii) allowing at least 90 wt % of the saccharide in the first portion of the starting material to react; iii) subsequently adding further portions of starting material to the reactor over time; and removing reaction product from the reactor.
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