- 专利标题: METHOD FOR PRODUCING POLYETHER CARBONATE POLYOLS
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申请号: US15527369申请日: 2015-11-16
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公开(公告)号: US20170321005A1公开(公告)日: 2017-11-09
- 发明人: Thomas Ernst Müller , Christoph Gürtler , Matthias Wohak , Jörg Hofmann , Carlson Torren
- 申请人: Covestro Deutschland AG
- 申请人地址: DE Leverkusen
- 专利权人: Covestro Deutschland AG
- 当前专利权人: Covestro Deutschland AG
- 当前专利权人地址: DE Leverkusen
- 优先权: EP14193601.3 20141118
- 国际申请: PCT/EP2015/076711 WO 20151116
- 主分类号: C08G65/26
- IPC分类号: C08G65/26 ; C08G64/34
摘要:
The invention relates to a method for producing polyether carbonate polyols, comprising the step of reacting alkylene oxide with carbon dioxide in the presence of an h-functional starter compound and double metal cyanide catalyst. The invention is characterized in that the method comprises the following steps: (α) optionally, pre-treating the double metal cyanide catalyst (DMC catalyst) at a temperature of 50 to 200° C. and/or reduced pressure (absolute) of 10 mbar to 800 mbar; (β) bringing the double metal cyanide catalyst in contact with suspension means, and furthermore, with alkylene oxide in the first reactor thus obtaining a first reaction mixture, and (γ) continuous added dosing of the first reaction mixture, alkaline oxide, and carbon oxide, and optionally, h-functional starter compound in a second reactor, wherein in at least one of the steps (β) or (γ), at least one h-functional starter compound is used, and wherein reaction products formed in step (γ) are continuously removed from the second reactor.
公开/授权文献
- US10138328B2 Method for producing polyether carbonate polyols 公开/授权日:2018-11-27
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