- 专利标题: METHOD FOR PREPARING DOUBLE-SEALED-END GLYCOL ETHER
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申请号: US15537928申请日: 2014-12-22
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公开(公告)号: US20170334818A1公开(公告)日: 2017-11-23
- 发明人: Youming NI , Wenliang ZHU , Hongchao LIU , Yong LIU , Zhongmin LIU , Lina LI , Shiping LIU , Hui Zhou
- 申请人: Dalian Institute of Chemical Physics, Chinese Academy of Sciences
- 申请人地址: CN Shahekou Dalian City
- 专利权人: Dalian Institute of Chemical Physics, Chinese Academy of Sciences
- 当前专利权人: Dalian Institute of Chemical Physics, Chinese Academy of Sciences
- 当前专利权人地址: CN Shahekou Dalian City
- 国际申请: PCT/CN2014/094535 WO 20141222
- 主分类号: C07C41/14
- IPC分类号: C07C41/14 ; B01J29/65 ; B01J29/40 ; B01J29/18 ; B01J29/70 ; B01J29/08
摘要:
Disclosed is a method for preparing a double end capped glycol ether, the method comprising: introducing into a reactor a raw material comprising a glycol monoether and a monohydric alcohol ether, and enabling the raw material to contact and react with an acidic molecular sieve catalyst to generate a double end capped glycol ether, a reaction temperature being 50-300° C., a reaction pressure being 0.1-15 MPa, a WHSV of the glycol monoether in the raw material being 0.01-15.0 h−1, and a mole ratio of the monohydric alcohol ether to the glycol monoether in the raw material being 1-100:1. The method of the present invention enables a long single-pass lifespan of the catalyst and repeated regeneration, has a high yield and selectivity of a target product, low energy consumption during separation of the product, a high economic value of a by-product, and is flexible in production scale and application.
公开/授权文献
- US10040739B2 Method for preparing double-sealed-end glycol ether 公开/授权日:2018-08-07
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