Invention Application
- Patent Title: A PROCESS FOR WORKING UP WATER CONTAINING 4,4'-DICHLORODIPHENYL SULFOXIDE AND/OR 4,4'-DICHLORODIPHENYL SULFONE AS IMPURITIES
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Application No.: US17775966Application Date: 2020-11-13
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Publication No.: US20220388949A1Publication Date: 2022-12-08
- Inventor: Stefan BLEI , Friedemann GAITZSCH , Christian SCHUETZ , Indre THIEL , Petra DECKERT , Jun GAO , Jessica Nadine HAMANN , Andreas MELZER
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen am Rhein
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen am Rhein
- Priority: EP19208797.1 20191113,EP20167479.3 20200401
- International Application: PCT/EP2020/082063 WO 20201113
- Main IPC: C07C315/06
- IPC: C07C315/06

Abstract:
The invention relates to a process for working up water containing 4,4′-dichlorodiphenyl sulfoxide and/or 4,4′-dichlorodiphenyl sulfone as impurities, comprising: (a) mixing the water containing 4,4′-dichlorodiphenyl sulfoxide and/or 4,4′-dichlorodiphenyl sulfone as impurities with an organic solvent in which 4,4′-dichlorodiphenyl sulfoxide and/or 4,4′-dichlorodiphenyl sulfone have a solubility of at least 0.5 wt % based on the amount of 4,4′-dichlorodiphenyl sulfoxide and/or 4, 4′-dichlorodiphenyl sulfone and organic solvent at 20° C., which forms a two-phase system with water and which can be stripped from water with a stripping gas and subsequently separating the obtained mixture into an aqueous phase and an organic phase, and (b) stripping the organic solvent from the aqueous phase with a stripping gas.
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