Invention Publication
- Patent Title: MESHED CATALYST BASED HIGH-YIELD PREPARATION AND REGENERATION METHOD FOR CARBON NANOTUBES AND HYDROGEN
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Application No.: US18013285Application Date: 2022-04-27
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Publication No.: US20240101428A1Publication Date: 2024-03-28
- Inventor: Huiyan ZHANG , Dongyang JIANG , Qingyu LIU , Ru HONG , Bo PENG , Rui XIAO
- Applicant: SOUTHEAST UNIVERSITY
- Applicant Address: CN Nanjing
- Assignee: SOUTHEAST UNIVERSITY
- Current Assignee: SOUTHEAST UNIVERSITY
- Current Assignee Address: CN Nanjing
- Priority: CN 2111351683.1 2021.11.16
- International Application: PCT/CN2022/089543 2022.04.27
- Date entered country: 2022-12-28
- Main IPC: C01B32/162
- IPC: C01B32/162 ; B01J23/86 ; B01J23/94 ; C01B3/26

Abstract:
A meshed catalyst based high-yield preparation and regeneration method for carbon nanotubes and hydrogen includes the following steps: step one, adding waste plastic into a low-temperature pyrolysis section, conducting slow heating, and continuously introducing nitrogen; step two, using a multilayer stainless steel mesh obtained through laminated pressing and vacuum sintering as a catalyst, introducing the volatiles into a high-temperature catalytic section, conducting a catalytic reaction under the action of a meshed stainless steel catalyst obtained through acid etching and calcination pretreatment, generating the carbon nanotubes on a surface of the catalyst, and meanwhile generating high-purity hydrogen; and step three, after temperature drop, conducting ultrasonic treatment on a stainless steel mesh after the reaction, achieving physical stripping of the carbon nanotubes from the stainless steel mesh, then placing the stainless steel mesh subjected to secondary calcination in a system for recycling, and regenerating the carbon nanotubes and the hydrogen.
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