Invention Publication
- Patent Title: METHOD FOR MANUFACTURE OF ISOPHORONEDIAMINE
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Application No.: US18564719Application Date: 2022-05-23
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Publication No.: US20240279155A1Publication Date: 2024-08-22
- Inventor: Martin SCHLODERER , Alfred KRAUSE , Andreas Edgar HERRMANN , Hannes Ferdinand GOUVERNEUR
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen am Rhein
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen am Rhein
- Priority: EP 177453.4 2021.06.02
- International Application: PCT/EP2022/063866 2022.05.23
- Date entered country: 2023-11-28
- Main IPC: C07C209/48
- IPC: C07C209/48 ; C07C209/86

Abstract:
The invention relates to a method for the production of IPDA comprising the steps of: V. converting IPN with ammonia and hydrogen to IPDA, VI. removing hydrogen and/or ammonia from the effluent from step I VII. separating the effluent from step II in one or more steps into (v) a fraction comprising an organic phase having a boiling point lower than IPDA (vi) a fraction comprising an aqueous phase having a boing point lower than IPDA; (vii) a fraction comprising IPDA (viii) a fraction comprising components having a boiling point higher than IPDA; and VIII. subjecting the fraction (ii) to one or more waste-water pretreatment steps, se-lected from the group consisting of evaporation, oxidation and adsorption.
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