发明授权
US3929707A Process for the production of pourable, pulverulent rubber-filler mixtures
失效
生产可倾倒,粉状橡胶填料混合物的方法
- 专利标题: Process for the production of pourable, pulverulent rubber-filler mixtures
- 专利标题(中): 生产可倾倒,粉状橡胶填料混合物的方法
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申请号: US48370974申请日: 1974-06-27
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公开(公告)号: US3929707A公开(公告)日: 1975-12-30
- 发明人: BERG GERHARD , NORDSIEK KARL-HEINZ
- 申请人: HUELS CHEMISCHE WERKE AG
- 专利权人: Huels Chemische Werke Ag
- 当前专利权人: Huels Chemische Werke Ag
- 优先权: DE2332796 1973-06-28
- 主分类号: C08L23/00
- IPC分类号: C08L23/00 ; C08C1/00 ; C08C2/06 ; C08J3/14 ; C08J3/16 ; C08J3/20 ; C08J3/215 ; C08K3/00 ; C08K3/04 ; C08K5/01 ; C08K5/17 ; C08L7/00 ; C08L21/00 ; C08L33/00 ; C08L33/02 ; C08L101/00 ; C08L9/04
摘要:
In a process for preparing discrete, finely divided, tack-free, pourable, powdery, filler-containing elastomer particles from an admixture of (a) an aqueous elastomer emulsion comprising (i) a solution of elastomer dissolved in a volatile, inert organic solvent having a boiling point below 100*C, (ii) an elastomer emulsifying amount of an alkylamine oxyalkylate surfactant, and (iii) water; and (b) an aqueous suspension or dispersion of a solid, finely divided elastomer filler, which comprises gradually introducing said admixture into an aqueous alkali silicate solution containing 2-20 moles of SiO2 per mole of said alkylamine oxyalkylate while maintaining said silicate solution at an acidic pH of 0.1-7 and simultaneously evaporating said volatile organic solvent to form said filler-containing elastomer particles, the improvement which comprises: EMPLOYING SAID ADMIXTURE OF (A) AND (B) IN THE FORM OF A STABLE, AQUEOUS EMULSION CONTAINING AN EMULSION-STABILIZING AMOUNT OF AN IONIC, WATER SOLUBLE PROTECTIVE COLLOID AND HAVING AN ALKALINE PH of 7-14.