Invention Grant
- Patent Title: Sulfurized calcium alkylphenolate compositions
- Patent Title (中): 硫酸烷基酚钙组合物
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Application No.: US500965Application Date: 1974-08-26
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Publication No.: US3969235APublication Date: 1976-07-13
- Inventor: Rodney L. Sung , Harry Chafetz , Benjamin H. Zoleski , Walter D. Foucher, Jr.
- Applicant: Rodney L. Sung , Harry Chafetz , Benjamin H. Zoleski , Walter D. Foucher, Jr.
- Applicant Address: NY New York
- Assignee: Texaco Inc.
- Current Assignee: Texaco Inc.
- Current Assignee Address: NY New York
- Main IPC: C10M163/00
- IPC: C10M163/00 ; C10M135/30 ; C10M159/12 ; C10M159/22 ; C10N10/04 ; C10N30/04 ; C10N30/10 ; C10N40/25 ; C10M1/38
Abstract:
A lubricating oil composition containing sulfurized calcium alkylphenolate detergent dispersant of superior resistance to oxidation prepared by (1) reacting at a temperature between 200.degree. and 425.degree.F. alkylphenol with a first addition of calcium alkoxyalkoxide to form a calcium alkylphenolate containing first reaction mixture utilizing between about 45 and 90 wt. % of the stoichiometric amount required to convert the alkylphenol to calcium alkylphenolate, (2) contacting the calcium alkylphenolate first reaction mixture with sulfur at a temperature between about 440.degree. and 460.degree.F. in the presence of between about 13 and 20 wt. % of a hydrocarbon lubricating oil based on step 2 second reaction mixture, and (3) contacting the second reaction mixture with a second addition of calcium alkoxyalkoxide at a temperature between about 350.degree. and 425.degree.F., said first and second addition totalling between about 100 and 120% of the stoichiometric amount of calcium alkoxyalkoxide to form said calcium alkylphenolate, said steps 1 and 3 being advantageously conducted while blowing their respective reaction mixtures with inert gas, step 2 being conducted while sequentially blowing step 2 reaction mixture with inert gas, carbon dioxide and inert gas.
Public/Granted literature
- US5647210A Driving device Public/Granted day:1997-07-15
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