- 专利标题: Process for the preparation of sulphonic acid chlorides
- 专利标题(中): 磺酰氯制备方法
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申请号: US941099申请日: 1978-09-08
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公开(公告)号: US4215071A公开(公告)日: 1980-07-29
- 发明人: Heinz U. Blank , Theodor Pfister
- 申请人: Heinz U. Blank , Theodor Pfister
- 申请人地址: DEX Leverkusen
- 专利权人: Bayer Aktiengesellschaft
- 当前专利权人: Bayer Aktiengesellschaft
- 当前专利权人地址: DEX Leverkusen
- 优先权: DEX2743542 19770928
- 主分类号: C07B61/00
- IPC分类号: C07B61/00 ; B01J31/00 ; B01J31/02 ; C07C67/00 ; C07C301/00 ; C07C303/02 ; C07C309/86 ; C07C143/26
摘要:
An improvement in a process for the preparation of the sulphonic acid chloride of the formula ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 are identical or different and denote hydrogen, a lower alkyl or cycloalkyl radical, halogen, nitro, aryl, aralkyl, aryl ether or a radical ##STR2## or wherein adjacent radicals R.sup.1 and R.sup.2 are linked to form a cycloaliphatic or aromatic carbocylic ring which is optionally substituted by a sulphonic acid chloride group by contacting a sulphonic acid of the formula ##STR3## wherein R.sup.1, R.sup.2 and R.sup.3 have the abovementioned meanings, with phosgene in the presence of a N,N-dialkylcarboxylic acid amide catalyst, the improvement wherein the process is carried out in the presence of a sulphonating agent.
公开/授权文献
- US6009442A Computer-based document management system 公开/授权日:1999-12-28