发明授权
- 专利标题: Process for the manufacture of N,N'-diacetylethylene diamine
- 专利标题(中): 制备N,N'-二乙酰乙二胺的方法
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申请号: US53033申请日: 1979-06-28
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公开(公告)号: US4219500A公开(公告)日: 1980-08-26
- 发明人: Gunter Roscher , Wilfried Pressler
- 申请人: Gunter Roscher , Wilfried Pressler
- 申请人地址: DEX Frankfurt am Main
- 专利权人: Hoechst Aktiengesellschaft
- 当前专利权人: Hoechst Aktiengesellschaft
- 当前专利权人地址: DEX Frankfurt am Main
- 优先权: DEX2828765 19780630
- 主分类号: C07C67/00
- IPC分类号: C07C67/00 ; C07C231/00 ; C07C231/02 ; C07C233/36 ; C07C103/44
摘要:
N,N'-Diacetylethylene diamine (DAED) is produced by first adding the stoichiometric amount of acetic acid (2 mols per mol of ethylene diamine) at least partially in the form of aqueous acetic acid to ethylene diamine, distilling off in a second step the water contained in the reaction mixture, adding acetic acid in excess to the remaining product, distilling off the aqueous acetic acid formed and recycling it into the first process step. The DAED remains as sump product after distillation of the acetic acid.
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