发明授权
US4286967A Double crystallization process to produce low organic, low silica soda
ash
失效
双结晶工艺生产低有机,低二氧化硅苏打灰
- 专利标题: Double crystallization process to produce low organic, low silica soda ash
- 专利标题(中): 双结晶工艺生产低有机,低二氧化硅苏打灰
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申请号: US163848申请日: 1980-06-27
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公开(公告)号: US4286967A公开(公告)日: 1981-09-01
- 发明人: Elwood F. Booth, Jr. , Rustom P. Poncha
- 申请人: Elwood F. Booth, Jr. , Rustom P. Poncha
- 申请人地址: NJ Morris Township, Morris County
- 专利权人: Allied Chemical Corporation
- 当前专利权人: Allied Chemical Corporation
- 当前专利权人地址: NJ Morris Township, Morris County
- 主分类号: C01D7/37
- IPC分类号: C01D7/37 ; C30B9/02
摘要:
A process for the production of low organic, low silica, anhydrous sodium carbonate comprising (a) calcining raw trona ore to produce crude sodium carbonate containing soluble and insoluble impurities, (b) admixing said crude sodium carbonate with a substantially saturated sodium carbonate solution to produce sodium carbonate monohydrate crystals containing insolubles and an impure sodium carbonate solution; (c) separating these monohydrate crystals and impurities; (d) dissolving the monohydrate crystals to produce a substantially saturated sodium carbonate solution and insolubles; (e) separating said solution from the insolubles; (f) evaporative crystallization of the separated saturated sodium carbonate solution to produce pure sodium carbonate monohydrate crystals; (g) optionally, subjecting the crystals recovered in step (f) to steps (d-f) once, but no more than once; (h) heating said monohydrate crystals to obtain low organic, low silica, anhydrous sodium carbonate product particles; and (i) optionally, repeating the sequence defined by steps (b-h) once, but no more than once is disclosed.
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