发明授权
US4316854A Process for the production of
bis-[0-(1-alkylthioethylimino)-N-methylcarbamyl]-N,N-sulfides
失效
制备双 - [O-(1-烷硫基乙基亚氨基)-N-甲基氨基甲酰] -N,N-硫化物的方法
- 专利标题: Process for the production of bis-[0-(1-alkylthioethylimino)-N-methylcarbamyl]-N,N-sulfides
- 专利标题(中): 制备双 - [O-(1-烷硫基乙基亚氨基)-N-甲基氨基甲酰] -N,N-硫化物的方法
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申请号: US156966申请日: 1980-06-06
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公开(公告)号: US4316854A公开(公告)日: 1982-02-23
- 发明人: Jean-Pierre Ledouble , Klaus Muller
- 申请人: Jean-Pierre Ledouble , Klaus Muller
- 申请人地址: NY Ardsley
- 专利权人: Ciba-Geigy Corporation
- 当前专利权人: Ciba-Geigy Corporation
- 当前专利权人地址: NY Ardsley
- 优先权: CHX5669/79 19790618
- 主分类号: C07C381/08
- IPC分类号: C07C381/08 ; A01N41/12 ; A01N47/24 ; C07C67/00 ; C07C325/00 ; C07C119/18
摘要:
A process for the production of bis-[0-(1-alkylthioethylimino)-N-methylcarbamyl]-N,N'-sulfides of the formula ##STR1## wherein R is a straight-chain or branched alkyl group of 1 to 5 carbon atoms, by reaction of a 0-(1-alkylthioethylimino)-N-methylcarbamate of the formula ##STR2## in the presence of a base, with sulfur dichloride or sulfur monochloride, in a solvent having a dielectric constant of 2.0 and a dipole moment of 0 to 1, is described.The bis-[0-(1-alkylthioethylimino)-N-methylcarbamyl]-N,N'-sulfides of the above formula possess insecticidal properties and are suitable in particular for controlling pests of cotton plants and bluebottles.