发明授权
- 专利标题: Continuous hydrolytic preparation of polylactams
- 专利标题(中): 多聚内酰胺的连续水解制备
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申请号: US581711申请日: 1984-02-21
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公开(公告)号: US4539391A公开(公告)日: 1985-09-03
- 发明人: Gunter Pipper , Rainer Theysohn , Franz Zahradnik
- 申请人: Gunter Pipper , Rainer Theysohn , Franz Zahradnik
- 申请人地址: DEX
- 专利权人: BASF Aktiengesellschaft
- 当前专利权人: BASF Aktiengesellschaft
- 当前专利权人地址: DEX
- 优先权: DEX3306906 19830226
- 主分类号: C08G69/00
- IPC分类号: C08G69/00 ; C08G69/16
摘要:
Polylactams are prepared continuously by a process in which a lactam containing from 1 to 25% by weight of water is heated in a prepolymerization zone under a pressure of from 1 to 10 bar at from 220.degree. to 280.degree. C. for 1 to 10 minutes, water being vaporized at the same time, with the proviso that the degree of conversion on emergence from the prepolymerization zone is not less than 85%, the prepolymer and the vapor are separated continuously, and the prepolymer is passed into a polymerization zone and is polymerized further under superatmospheric pressure at from 240.degree. to 290.degree. C.
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