发明授权
US4584413A Purification of tertiary butyl hydroperoxide containing primary and secondary alkyl hydroperoxide contaminants 失效
含叔丁基氢过氧化物的叔烷基氢过氧化物污染物的纯化

Purification of tertiary butyl hydroperoxide containing primary and
secondary alkyl hydroperoxide contaminants
摘要:
This invention relates to the purification of tertiary butyl hydroperoxide containing minor amounts of primary and secondary alkyl hydroperoxide contaminants obtained by the oxidation of isobutane by contacting the tertiary butyl hydroperoxide with at least about 2 milliequivalents per gram of total hydroperoxide present of a hydroxide or an oxide of an alkali metal or alkaline earth metal in aqueous solution and recovering the desired tertiary butyl hydroperoxide containing substantially reduced concentrations of primary and secondary alkyl hydroperoxide contaminants.
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