发明授权
- 专利标题: Method and system for producing carbon fibers
- 专利标题(中): 生产碳纤维的方法和系统
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申请号: US742103申请日: 1985-06-05
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公开(公告)号: US4610860A公开(公告)日: 1986-09-09
- 发明人: Charles K. Mullen
- 申请人: Charles K. Mullen
- 申请人地址: CA Newport Beach
- 专利权人: Hitco
- 当前专利权人: Hitco
- 当前专利权人地址: CA Newport Beach
- 主分类号: D01F9/22
- IPC分类号: D01F9/22 ; D01F9/32
摘要:
High tensile carbon fibers are provided with a high yield process in which, after oxidation of a precursor, the fibers are first precarbonized in an inert atmosphere to to about 600.degree. C. while imparting 5-10% stretch. In precarbonizing, the fibers are initially heated in a sweeping manner with substantial volumes of hot inert gas which is extracted along with products of decomposition before the fibers are cooled to a low, non-reactive exit temperature. The arrangement minimizes redeposition of tars on the fibers and stretches the fibers in a range in which substantial off-gassing occurs. Thereafter the fibers are finally carbonized at a higher temperature with a different tension being applied, to provide a more reliable less sensitive process that enables oxidation to be effected more rapidly.
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