发明授权
- 专利标题: Glycerol distillation process
- 专利标题(中): 甘油蒸馏工艺
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申请号: US664902申请日: 1984-10-26
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公开(公告)号: US4655879A公开(公告)日: 1987-04-07
- 发明人: Rolf Brockmann , Lutz Jeromin , Wilhelm Johannisbauer , Helmut Meyer , Otto Michel , Juergen Plachenka
- 申请人: Rolf Brockmann , Lutz Jeromin , Wilhelm Johannisbauer , Helmut Meyer , Otto Michel , Juergen Plachenka
- 申请人地址: DEX Duesseldorf
- 专利权人: Henkel Kommanditgesellschaft auf Aktien
- 当前专利权人: Henkel Kommanditgesellschaft auf Aktien
- 当前专利权人地址: DEX Duesseldorf
- 优先权: DEX3339051 19831028
- 主分类号: B01D3/14
- IPC分类号: B01D3/14 ; B01D3/32 ; C07C27/00 ; C07C29/80 ; C07C29/88 ; C07C31/22 ; C07C67/00 ; B01D3/34 ; B01D1/22
摘要:
An improved process for purification of glycerol obtained from natural sources comprising alkalizing a glycerol-containing crude mixture in the presence of air for oxidation, evaporating the mixture in a thin-layer evaporator with redistillation of the residue, rectification and reevaporation in a packed column characterized by low-pressure-loss plates with a falling-film evaporator designed for internal and external partial condensation and to separate off unwanted constituents of the mixture, bleaching the product with activated carbon and separating the bleach in known manner.